Abstract

This study evaluated the effects of thermocycling and staining on the optical behavior, chemical stability, and surface morphology of three commercial dental composites manufactured using different polymerization protocols: a light-cured composite (Omnichroma, OMNI) and two digital light-processed (DLP) 3D-printed composites intended for permanent (SprintRay CROWN, SPRINT) and temporary (GC Temp PRINT, TEMP) clinical applications. Disc-shaped specimens were subjected to thermocycling (0, 5000, 10,000, and 30,000 cycles) and immersion in coffee, Coca-Cola, or red wine for 1 and 7 days. Color change (ΔE00) and translucency parameter (TP) were determined spectrophotometrically, while Fourier-transform infrared spectroscopy (FTIR) and atomic force microscopy (AFM) were employed to assess the polymerization efficiency (expressed as the relative conversion index) and surface morphology, respectively. Thermocycling induced material-dependent changes in color stability and translucency. After 30,000 cycles, ΔE00 values reached 2.77 ± 0.89 for OMNI, 0.74 ± 0.34 for SPRINT, and 3.30 ± 0.89 for TEMP. SPRINT maintained the highest TP values throughout the aging protocol, ranging from 26.09 ± 0.33 to 23.81 ± 1.93, whereas OMNI and TEMP exhibited lower TP values. The most favorable optical performance and the highest resistance to beverage-induced coloration were detected for SPRINT, whereas TEMP showed the greatest susceptibility to aging- and staining-induced optical degradation. Red wine and coffee produced substantially greater color changes and reductions in translucency than Coca-Cola. AFM analysis demonstrated progressive surface degradation and increased roughness following prolonged thermocycling, highlighting the significant influence of material composition and manufacturing protocol on the long-term optical stability of the investigated dental composites.

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